SPEC Engineers & Consultants Pvt. Ltd.  
 

Franken

 
   
 

Franken

 
 

Phase Seperators

 
  Liquid / Liquid Phase Separation  
     
 
Liquid Phase Separation   Liquid Phase Separation
 
     
 
Liquid Phase Separation   Liquid Phase Separation
 
     
  Why Phase Separators?
Phase separators remove droplets with diameters >0.1µm from liquid/ liquid dispensions. The resulting improvement in the purity of liquid recovered from both dispersed and continuous phases increases product quality and reduces the need for downstream treatment. FRANKEN Phase separators thus increase profits significantly as the investments and operating costs are low.
 
     
  Phase Separators ('Separators') : FRANKEN designed separators guarantee a very high performance because of application of state-of-the-art design rules based on empirically verified CFD design models and use of the proprietary range of high performance internals.  
     
  Design philosophy : Droplete- droplet coalescence on microfibre, wire mesh and profile surfaces allows large droplets ( d> 1,000 µm) to form quickly and efficiently. As these droplets flow through the phase separator vessel, density differences cause them to migrate to the liquid interface under the influence of gravity.
Since coalescence is a mechanical separation process, it cannot remove the dissolved liquids.
 
     
  Perfect Separation : FRANKEN phase separators are designed for optimal coalescence in separating organic or aqueous droplets.To design each separator the major parameters are
1. Droplet size distribution at the inlet
2. Wetting behavior of the two liquids
3. Interfacial tension.
 
     
  Separation task defines the phase separation procedure :  
  Droplet Size defines the type of SEPERATOR  
 
PT phase Separator
Fine droplets >0.1µm
MPT phase Separator
medium droplets >10µm
PTG phase Separator
coarse droplets >50µm
Coalescence process - Droplet formation and separation
In Microfibre beds

Flow guides the fine droplets to the micrifibers

Droplet-droplet coalescence (collection of droplets) at the fiber cross points

Displacements of coarse droplets (d >1,000µm) at the fiber bed
At profile surfaces

Density difference guides the droplets to the profile surfaces

Droplet-droplet coalescence at the profile surfaces

Displacements of coarse droplets ( d > 1,000µm) at certain profile areas
At the interface

Coarse droplets shift to the interface under gravity

Droplet- droplet coalescence at the interface
 
     
  Process Conditions :  
 
  Units PT MPT PTG
Density difference Kg/m3 >10 >50 >150
Viscosity of continuous phase Mpas <500 <20 <5
Viscosity of dispersed phase Mpas <500 <1,000 <2,000
Interfacial tension( no surfactants) mN/m >2 >2 >2
Maximum concentration of dispersed phase vol% <10 Any Any
Differential pressure (clean/ maximum) bar g <0.05/1.5 <0.02 <0.02
Solid particles µm <5 <25  
 
     
  Application :  
 
PT Phase separator MPT Phase separator PTG Phase separator
Product treatment
  - water from silicone oil
  - water from polycarbonate
Biodiesel
  - Glycerine from methyl ester
  - Fatty acid from glycerine water
Process enhancement
  - Water from cumene
  - Raffinate from methyl pyridine
Process enhancement
  - Rh solution from aldehyde
  - extractant from Cs solution
  - benzene fron hydrochloric acid
Hydrocarbons from waste water
Process enhancement

  - Caustic soda from vinyl chloride
  - Silicone oil from hydrochloric acid
Capacity Enhancement
  - Reservoir water from crude oil
  - MCB/DCM from waste water
  - Hydrocarbon from water
 
     
  Benefits :
• Very high separation efficiency
• Separation down to solubility limit
• Low pressure drop (<50 mbar)
• Wide selection of material
• Low operating costs
• Low maintenance
• Customized engineering and manufacture
 
     
  Focus on the Environment :
• Our technologies contribute to ecological sustainability and lower energy use.
• Modular and extensible design helps to make phase separaters future- proof.
• At the end of there operating lives, the internals can be refurbished or recycled.
 
     
 
 
For laboratory and pilot plant scale testing, we are able to manufacture phase Separation elements of smallest dimensions for subsequent scale-up (e.g. Ø 50 mm)
 
     
  Referance Installations  
 
     
  2x 4-stage ion-exchange system for the purification of Biodiesel;
Capacity: 20 MMgy
Locations:
Europe: Austria, Germany, Netherlands,
USA : Arkansas, California, Missouri, Texas
  PT phase separator for the separation of watery phase from RME;
Capacity: 25 m³/h; 35 MMgy
Locations:
Europe: Austria, Germany, Great Britain
 
         
     
  MPT phase separator for the separation of glycerine from methyl ester;
Capacity: 17,5 m³/h (4,600 gal/h),
Separation efficiency: all droplets > 25 µm
Locations:
Asia: India, Malaysia, Singapore Australia, USA
Europe: France, Germany, Great Britain, Spain
  PT phase separator for the separation of glycerine water from methyl ester;
Capacity: 52 m³/h; 80 MMgy
Locations:
Australia
Europe: Austria, Germany, Great Britain
 
 
     
     
 
  Designed & Manufactured By
Franken Filtertechnik KG
Max – Planck – Strasse 7
50354 Huerth
Germany
Tel +49 (0) 2233 9744-0
Fax +49 (0) 2233 97440-40
Web : www.frankenfilter.com
Email : info@frankenfilter.com
  Represented in INDIA by
SPEC Engineers & Consultants Pvt. Ltd.
2/86, WHS, Kirti Nagar
New Delhi – 110015
India
Tel +91 11 4142 0206 , 2541 3597
Fax +91 11 2519 3715
Web: www.specengineers.com
Email: info@specengineers.com